ISOLASI DAN KARAKTERISASI INOSITOL DARI BIJI JAGUNG (ZEA MAYS SACCHARATA) DENGAN METODE ULTRASOUND -ASSISTED SOLVENT EXTRACTION DAN GAS CHROMATOGRAFY MASS SPECTROMETRY (GCMS)

Penulis

  • Andi Muhamad Iqbal Akbar Asfar
  • Setyo Erna Widiyanti

Abstrak

This research was simply isolated inositol and physic characterisation from sweetcorn (Zea Mays Saccharata). Extractedused Ultrasound - Assisted Solvent Extraction (high frequency signal of 20 kHz). Comparation solvent this research(C2H5OH dan H2O) through variances ethanol dan water as solvent consist of 70%, 75%, 80%, dan 85% for ethanolvariances and 5 gr, 10 gr, 15 gr, dan 20 gr for variances of water as solvent through watered down until 100 ml in beakerglass. Yield extracted as isolated in 75% of ethanol solvent is 76%. Water content and ash content from sweetcorn seedeach of gave result are 76,48% and 0,7979%. Isolated after vaporated characterized with Gas Chromatografy MassSpectrometry (GCMS), the results were not able to detect the presence of Inositol (myo-inositol), but detected the othermonosaccharide content of 2-Furaldehyde. It is estimated that inositol (myo-inositol) is still detectable as 2-Furaldehydewith a very small percentage of abundance.

Referensi

Ayunda, Nesia. 2014. Pertumbuhan Dan Hasil Tanaman Jagung Manis (Zea Mays Saccharata Sturt.) Pada Beberapa

Konsentrasi Sea Minerals. Fakultas Pertanian, Universitas Taman Siswa, Padang.

Daneluti, André Luis Máximo & Matos, Jivaldo do Rosário. 2013. Study of thermal behavior of phytic acid. Brazilian

Journal of Pharmaceutical Sciences, Vol. 49, No. 2, April-Juni 2013, Hal. 275-283.

Indyk, Harvey E., Saldo, Sheila C., White, Peter M., Dole, Mumtaz N., Gill, Brendon D., & Woollard, David C. 2016.

The Free And Total Myo-Inositol Contents Of Early Lactation And Seasonal Bovine Milk. International Dairy

Journal 56 (2016), hal. 33-37.

Jian-Rui Liu, Yi-Na Guo, Wei-Dong Huang. 2011. Formation Process and Properties of Phytic Acid Conversion

Coatings on Magnesium. Journal of Surface Engineered Materials and Advanced Technology, 2011, 1, hal. 15-21.

Joy, Amitha & Balaji, S. 2015. Drug-Likeness of Phytic Acid and Its Analogues. The Open Microbiology Journal, 2015,

Vol. 9, Hal. 141-149.

Kerovuo, J. 2000. A Novel Phytase From Bacillus: Characterization And Production Of The Enzyme. Ph.D dissertation,

Univ. Helsinki, Finland.

Lee A, H. S & G. A. Coates. 2000. Quantitative Study Of Free Sugars and Myo-Inositol In Citrus Juices By HPLC and

A Literature Compilation. Journal of Liquid Chromatography & Related Technologies 23(14), hal. 2123–2141.

McDonald, L. W., Goheen, S. C., Donald P. A., & Campbell, J. A. 2012. Identificat Ion And Quantitat Ion Of Va Rious

Inositols And O-Methylinositols Present In Plant Roots Relate D to Soybean Cyst Nemat Ode Host Stat US.

NEMATROPICA Vol. 42, No. 1, 2012, hal. 1-8.

Solé, Aran., Neumann, Hannah., Niedermaier, Sophia., Cabezaa Luisa F., & Palomo, Elena. 2014. Thermal Stability

Test Of Sugar Alcohols As Phase Change Materials For Medium Temperature Energy Storage Application. Energy

Procedia 48, 2014, hal. 436 – 439.

Winarto, W.P. 2004. Memanfaatkan Tanaman Sayur untuk Mengatasi Aneka Penyakit. Tangerang: AgroMedia Pustaka.

Diterbitkan

2018-08-28

Terbitan

Bagian

KIMIA, LINGKUNGAN, BIOKIMIA DAN BIOPROSES